vacuum prepared sample 中文意思是什麼

vacuum prepared sample 解釋
真空制備的試樣
  • vacuum : n （pl vacuums vac ua ）1 真空；空處，空虛，空白。2 〈美口〉吸塵器（＝ vacuum cleaner）。vi vt 〈...
  • prepared : adj. 1. 有準備的，準備好的。2. 精製的，特別處理過的。adv. -ly
  • sample : n 1 樣品，貨樣。2 標本；榜樣，實例。3 【統計】典型取樣，抽檢查。4 【電訊】信號瞬時值。5 【冶金】 ...
  1. The sample composition was analyzed by means of tg and x - ray diffraction. the following conclusions can be drawn from the experiments : given conditions, the sample powder that has the same xrd data as the standard fetioa can be gotten when use any method mentioned above ; the key in synthesis is to avoid the oxidation of fe2 +, so the whole process should performed under vacuum or neutral atmosphere, samples used by this study were prepared under nitrogen atmosphere ; the heat - treated time and temperature have some influence on the sample powder, results show that the proper time and temperature is 120 minutes and 1100 respectively

    研究結果表明：在合適的反應條件下，用上述三種合成方法都能得到xrd數據與標準fetio _ 3物相基本吻合的粉體；合成反應需要克服的主要問題是防止體系中fe ~ （ 2 + ）的氧化，因此，整個反應必須在真空或者非氧化性氣體保護下進行，本研究需要的樣品是在高純從保護下合成的；煅燒的時間和溫度對最終的產物也有一定的影響，研究發現：合理的煅燒時間和溫度分別為120分鐘和1100 。
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