縮醛反應 的英文怎麼說
中文拼音 [suōquánfǎnyīng]
縮醛反應
英文
aldolisation-
Furbenicillin sodium, a known semi - synthetic ureide type of antibiotic firstly marketed in china, was synthesized from starting material 2 - furaldehyde via six steps including oximation reaction, beckmann rearrangement, isocyannuration, amination, condensation and salification etc
摘要以呋喃甲醛為起始原料,經厲化、貝克曼重排、異氰脲酸化、氨基化、縮合和成鹽6步反應,合成了酰脲類青霉素抗生素呋布西林鈉。Scheme 1. condensation of pyrrole and benzaldehyde
圖式1吡咯與苯甲醛的縮合反應。Under acid condition open chaining crown ether diaromatic aldehyde can react, and they will synthesize a compound of chaining crown ether diaromatic aldehyde thiosemi - carbazone kind
摘要鏈狀冠醚二芳醛在酸性條件下與氨基硫脲反應,合成了鏈狀冠醚二芳醛縮氨硫脲類化合物。An one - pot process including direct condensation of ethyl isodehydracetate and hydrocitronellal, followed by decarboxylation, isomerization and isomer resolution, was developed for practical preparation of zr juvenile hormone analogue series with high content of effective component
以異脫氫乙酸乙酯與甲氧基香茅醛直接縮合為起點,將縮合、脫羧、異構化、 (順、反)異構體拆分等採用多步反應連續一鍋法的操作方法,成功地得到高有效含量的zr型保幼激素類似物。1. two kinds of organic hydrate thermochromic material are synthesized. the compounds are found that they show thermochromic mechanics : p - nitrophenol 1. 5h2o and p - nitroaniline 3h2o are conjugated between phenyl rings and water molecules. they are characterized by charge - transfer interactions with counterions
3 、通過室溫/低熱固相反應合成了雙席夫堿聯苯胺縮二水楊醛以及該雙席夫堿與nicl _ 2 ? 6h _ 2o的配合物。Synthesis of pentaerythritol diacetals from aldehydes and ketones under microwave irradiation
催化下微波促進芳香醛與環酮的縮合反應Cratoneuron taihangense musci : amblystegiaceae, a new species from hebei province, china
二甲基甲酰胺二異丙基縮醛對羧酸酯化反應的研究Chitosan ' s modification - study of condensation reaction with n - butyl aldehrde
殼聚糖與正丁醛縮合反應的研究In this paper, 1, 1 - diacetate was synthesized from furfural and acetic anhydride by acidic bentonite friendly to environment as catalyst with excellent yield ( 87. 6 % )
摘要利用對環境友好的酸性皂土做催化劑,糠醛與乙酸酐發生縮合反應合成了1 , 1 -二乙酸酯,產率高達86 . 6 % 。The traditional catalyst used in acetal ( ketal ) synthetic reaction is strong inorganic acid. but there is some limits to its use because of its side reaction, strong erosion and liability to pollute the environment. molybdophosphoric acid is used as catalyst and three condensation products are prepared through the direct reaction of aldehydes ( ketones ) and ethylene. in addition, several elements of affecting the reaction is researched. it is proved that molybdophosphoric acid is very active as catalyst in less addition, the product yield is quite high and the quality of reuse is quite good
縮醛(酮)合成反應的傳統催化劑為無機強酸,但由於副反應多、腐蝕性強和易污染環境等缺點,其使用受到限制.用磷鉬酸為催化劑,通過醛(酮)與乙二醇直接反應得到了三種縮合產物.對影響反應的諸因素進行研究,結果表明,用磷鉬酸作催化劑,用量小,活性高,產品收率較高,且重復使用性能較好Abstract : the traditional catalyst used in acetal ( ketal ) synthetic reaction is strong inorganic acid. but there is some limits to its use because of its side reaction, strong erosion and liability to pollute the environment. molybdophosphoric acid is used as catalyst and three condensation products are prepared through the direct reaction of aldehydes ( ketones ) and ethylene. in addition, several elements of affecting the reaction is researched. it is proved that molybdophosphoric acid is very active as catalyst in less addition, the product yield is quite high and the quality of reuse is quite good
文摘:縮醛(酮)合成反應的傳統催化劑為無機強酸,但由於副反應多、腐蝕性強和易污染環境等缺點,其使用受到限制.用磷鉬酸為催化劑,通過醛(酮)與乙二醇直接反應得到了三種縮合產物.對影響反應的諸因素進行研究,結果表明,用磷鉬酸作催化劑,用量小,活性高,產品收率較高,且重復使用性能較好The pentaerythritol diacetals were effectively synthesized through condensation reaction of pentaerythritol with aldehydes and ketones promoted by zirconium sulfate - silica gel under microwave irradiation
摘要微波輻射硫酸鋯矽膠催化季戊四醇與醛、酮縮合反應,高收率制得了雙縮醛和雙縮酮化合物。The promotion action of ionic liquid as an accelerant in synthesizing benzaldehyde ethanediol acetal and benzaldehyde propanediol acetal was studied
摘要以離子液體為促進劑,強酸性聚苯乙烯732催化了苯甲醛與兩種二元醉的縮醛反應。It was found that before the plating, there is section time to gestating, that we call the " gestating time " and the plating was ended spontaneously after some time, named " plating time ". the analysis of the solution after plating indicated that the too much decrease of ph value results in the reaction to be stopped. the plating time was shortened when the ph and the temperature of the bath were increased
結果表明,鍍液ph浙江大學碩士學位論文范啟義2003年3月摘要值、施鍍溫度提高,由於反應的速度加快,使反應時間縮短;硫酸銅濃度提高,有助於加快反應速度,從而縮短反應時間; edta濃度提高,使鍍液穩定性升高,對反應時間的影響等效于硫酸銅濃度的降低;而甲醛濃度提高,雖然反應的速度加快,但由於可用於還原的量增加,因此反應時間增加;裝載量提高,因能鍍覆的表面積增加,使反應時間縮短。Fluoroalkyl acetic acids were converted to their corresponding carbonyl chlorides, which was then reacted with o - amino benzaldehyde and ammonia gas to give 3 - ( 1 - iminofluoroalkyl ) - 1h - qunolin - 2 - ones in moderate yields
摘要用2 -氟烷基乙酸為初始原料,用氯化亞碸或五氯化磷將其轉化為相應的酰氯,後者在室溫與鄰胺基苯甲醛縮合,通入氨氣迴流反應得到3 - ( 1 -亞胺基氟烷基) 1h -喹啉2 -酮類化合物,產率中等。In the course of oxidation, reaction temperature should rise step by step, and in the late stage, reduced pressure distillation should follow so that the concertration of glyoxalic acid can rise and production rate of allantoin can rise up to 40 %
在氧化反應的過程中逐步地提高反應溫度,反應後期進行減壓濃縮,提高了乙醛酸的濃度,縮短了氧化時間,並使尿囊素產率達到40 % 。分享友人