試劑的純度 的英文怎麼說
中文拼音 [shìjìdechúndù]
試劑的純度
英文
purity of reagents- 試 : 名詞(古代占卜用的器具) astrolabe
- 劑 : Ⅰ名詞1 (藥劑; 制劑) a pharmaceutical or other chemical preparation 2 (某些有化學作用的物品) a...
- 的 : 4次方是 The fourth power of 2 is direction
- 純 : 形容詞1 (純凈; 不含雜質) pure; unmixed 2 (純粹; 單純) simple; pure and simple 3 (純熟) skil...
- 度 : 度動詞[書面語] (推測; 估計) surmise; estimate
- 試劑 : [化學] reagent; agentia; analoids試劑廠 chemical reagent works
- 純度 : fineness; pureness; purity; purity quotient; rate of purity
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In this thesis, the development of emulsion polymerization theory and related new technologies are comprehensively reviewed, and the synthetic technologies of acrylate latex modified by organosilicon both at home and abroad are also reviewed. based on the current development and research in this field, attentions of this study are focused on three ways for preparing novel acrylate latexes modified by organosilicons, that is, 1 ) the acrylate monomers are copolymerized with unsaturated silicons by emulsion copolymerization ; 2 ) a new latex with microphase separation morphology is synthesized, which shows a core - shell structure character ; 3 ) soap - free polymerization is explored for preparing a higher - performance latex using an unsaturated silicon monomer, different acrylates and a reactive emulsifier. by using techniques of delaying addition of organosilicon monomer and a hydrolysis inhibitor, the hydrolysis and condensation of 3 - ( trimethoxysilyl ) propyl methacrylate during polymerization can be effectively prevented, as a result, organosilicon content in the macromolecular chain is increased
同時採用有機硅單體延遲滴加及添加水解抑制劑等技術,有效防止了-甲基丙烯酰氧基丙基三甲氧基硅烷在乳液聚合過程中的過渡水解及縮合反應,提高了聚合物大分子鏈中有機硅鏈節的含量;利用紅外光譜與差示掃描量熱儀對產物分子結構進行了表徵,並通過對共聚產物力學和吸水率的測試,證實了本研究所制備的有機硅改性丙烯酸酯共聚物具有比純丙烯酸酯聚合物更優良的力學及耐水性能;從分子設計角度出發,利用醇解反應合成出水解、縮合反應速率較慢的兩種新型不飽和有機硅單體: ?甲基丙烯酰氧基丙基三乙氧基硅烷和?甲基丙烯酰氧基丙基三異丙氧基硅烷;利用核磁共振對新型硅烷單體結構進行了證實;研究表明利用新型硅烷單體可以制備出高硅烷含量的有機硅改性丙烯酸酯乳液,且其聚合產物具有較高的力學及耐水性能。We have prepared a series of neodymium binary / ternary complexes, such as nd ( acac ) 3 ' 2h2o, nd ( tfa ) 3 ' 2h2o, nd ( hfa ) 3 ' 2h2o, nd ( dbm ) 3 ' h2o, nd ( acac ) 3phen, nd ( tfa ) 3phen, nd ( hfa ) 3phen, nd ( dbm ) 3phen, nd ( tta ) 3 ( tppo ) 2, nd ( hfa ) 3 ( tppo ) 2, nd ( acac ) 4hpy, nd ( tta ) 4hpy and ndq3. the effects of organic ligands, synergistic coordination agents and different substitution groups for - diketones on effective line width and photoluminescence intensity of neodymium complexes were investigated. the photoluminescence spectra indicate that synergistic coordination agents can shield neodymium ion and impede water molecules penetrating into inner coordination shell to satisfy large coordination number of nd3 + during hydrous synthesis process, so the luminescence intensity of neodymium ternary complexes is stronger than that of neodymium binary complexes
發光光譜研究表明,由於協同試劑的參與,屏蔽了水分子參與配位,降低了羥基( oh )對釹離子激發態能級~ 4f _ ( 3 2 )的猝滅,三元配合物的熒光強度均比二元配合物強,其中配合物nd ( tta ) _ 3 ( tppo ) _ 2在1340nm處的熒光強度最強,適合作為摻雜的光學活性物質,來制備有源光波導材料;在有水工藝條件下,單純地氟化配體未必能提高釹配合物的近紅外發光性能。Phosphorus pentoxide is usual material and reagent in chemical industry, this product is widely used in the industries of medicine, coating auxiliaries, printing and dyeing auxiliaries, anti static additive, titanate coupling agent, phosphorus oxychloride, chemical. mainly used in producing high purity phosphoric acid, used as desiccant of gas and liquid, dehydrant of organic synthesis
五氧化二磷是化學工業中常見的原料和試劑,本品廣泛用於醫藥,塗料,印染,化工等行業,主要用於製造高純度磷酸,用作氣體和液體乾燥劑,有機合成的脫水劑,以及有機磷酸酯的制備。The degrees of crystallinity of pure ptfe under the different conditions of water cooling, air cooling and furnace - varying cooling were made comparison by xrd. the thermal stability of pure ptfe and solid lubricant was analyzed by dsc - tg ; the composition and valence state of elements in the surface of carbon fiber, solid lubricant before and after friction test and lubricant transfer film were characterized by xps ; the frictional property of solid lubricant was tested by pin and disk test rig. the frictional wear property of solid lubricant between embedded bearing sleeve and steel axle friction pair ring was tested by special simulate test machine, the hardness of solid lubricant was tested by pm ; the compression strength of solid lubricant was tested by material test machine
用sem表徵原料微觀結構、摩擦表面及潤滑轉移膜表面形貌:用xrd進行原料物相分析,及比較水冷卻、空氣冷卻、隨爐冷卻三種工藝條件下的純聚四氟乙烯樹脂的結晶度;用dsc - tg分析純聚四氟乙烯樹脂及固體潤滑劑的熱穩定性;用xps表徵碳纖維表面、固體潤滑劑摩擦前後表面、潤滑轉移膜表面的元素組成、價態變化;用銷盤式摩擦磨損試驗機對固體潤滑劑進行摩擦性能測試;採用專用的臺架模擬試驗機對固體潤滑劑鑲嵌軸承套與鋼軸摩擦副間的摩擦磨損性能進行測定;用萊次偏光顯微鏡( pm )測試固體潤滑劑的硬度;用材料試驗機測試固體潤滑劑的抗壓強度等。The results indicated that the dimension, shape and purity of base material could meet the functional demand of solid lubricant ; the thermal decomposition temperature of ptfe resin exceeds 400 c, but organic and inorganic packing filler added in ptfe made the water absorption rate of composite material increased, melting temperature and decomposition temperature decreased, in the meanwhile oxidative decomposition reaction was accompanied ; polar groups such as c = o, c - o - c and so on in the carbon fiber surface is advantageous to increase compatibility with other components and interlayer shearing strength ; uniform design experimental method could help to find the relationship between formula and frictional property by relatively small tests. the developing trend of each formula ' s friction coefficient could be showed by fitting curve ; the friction coefficient with no copper powder or graphite in formula was relatively big. this fact showed that copper powder and graphite should be used cooperatively ; it was found that when the ratio of copper powder to graphite by weight is 15 : 60, 30 : 30 - 40 and 60 : 15 - 30 respectively, the friction coefficient was relatively small. the degree of crystallinity of pure ptfe reached maximum by air cooling and the abrasion loss also reached maximum among three ones ; at the same time, the abrasion loss of solid lubricant sample was also the biggest among three ones ; when solid lubricant matched with 45 # steel axle or gcrl5 steel axle, lubricant transfer film could be formed on metal surface, thus direct contact between the surface of metal friction pair rings was reduced. their working life was elongated extremely ; there was mainly much graphite, a little ptff, moo3, feso4, cus and so on in lubricant transfer film
試驗結果表明:所選原料的尺寸、形狀及純度可滿足固體潤滑劑的性能要求;聚四氟乙烯樹脂熱分解溫度超過400 ,但在ptfe中加入無機填料會使復合材料吸水率提高,熔融溫度及分解溫度降低,且伴有氧化分解反應;碳纖維表面含有c = o及c - o - c等極性基團,有利於提高其與其它組分的相容性,提高層間剪切強度;均勻設計試驗方法能夠用較少的試驗次數找出配方與摩擦性能間的關系,擬合曲線基本能表示各配方的摩擦系數發展趨勢;配方中不加銅粉或不加石墨,其摩擦系數均較高,說明銅粉和石墨應該配合使用;當銅粉15份、石墨60份時,銅粉30份、石墨30 - 40份時,銅粉60 、石墨15 - 30份時,摩擦系數均具有較低值;純聚四氟乙烯樹脂在空氣冷卻時結晶度最大,磨損量也是三者中最大的;同時,固體潤滑劑試樣在空氣冷卻時的磨損量也是三者中最大的:不論是固體潤滑劑與45 #鋼軸配副或是固體潤滑劑鑲嵌入銅套后與gcr15鋼軸配副,在金屬表面均可形成潤滑轉移膜,從而減少金屬摩擦副表面間的直接接觸,大大延長其使用壽命;轉移膜中主要含有較多的石墨、少量聚四氟乙烯、 moo 。Experimental results show that the order of fluoride salt being put in and flux type also influences the phases constitution, morphology, distribution and absorbent rate of ti and b. the experiments on remelting master alloys and al or al alloys at a certain temperature range show that the phases constitution and size have a remarkable heredity
試驗結果表明,不同的氟鹽加入順序和熔劑種類的不同也直接影響著中間合金中化合物的相組成、形態、分佈以及中間合金中ti 、 b的實收率等。在用純鈦顆粒法制備中間合金時,熔煉溫度的改變只能影響tial _ 3晶體的尺寸大小,而無法改變其形態。Extraction of large - fragment genomic dna in order to gain dna template of pcr amplification ( long pcr amplification and salvage pcr amplification ) which was high purity and large fragment, three methods were used to extract genomic dna of bacillus subtilis, i. e. low melting - point agarose embedding method, sds - proteinase k - phenol chloroform extraction method and bacterial genomic dna extraction kit method. the genomic dna of bacillus subtilis were gained by these methods, and the operated programs of the methods were improved. the results showed that the genomic dna extracted by low melting - point agarose embedding method were obviously biggest than that of another two methods
大片段基因組dna的提取為了獲得用於pcr擴增(長距離pcr擴增和分段pcr擴增)的高純度、大片段(至少為pcr產物長度的4倍)的dna模板,應用三種方法:低熔點瓊脂糖包埋法, sds -蛋白酶k -酚氯仿抽提法和細菌基因組dna提取試劑盒法,分別提取獲得了枯草桿菌基因組dna ,並對3種方法的操作程序進行了不同程度的改進,結果表明:低熔點瓊脂糖包埋法提取的基因組dna片段明顯大於后兩種方法,採用0 . 5瓊脂糖凝膠電泳3h ,仍然跑不出加樣孔。Different liquids, pure water and hydrochloric acid, nitric acid and aqua regia were tested with icp - ms analysis to collect borehole nanoscale material, and concentrations of elements in varied liquids were determined
摘要利用等離子體質譜技術,對已知礦區井下進行了純水和不同濃度的鹽酸、硝酸和王水等液態捕集劑的捕集吸附性能試驗研究,獲得了不同液態捕集劑中元素含量隨濃度變化的規律。This article confirmed the grafting efficiency of starch grafted to acrylic acid and the structure of starch and its grafted matter through the separation, purification and analysis tests to the grafted copolymer and the grafted forked - chain matter produced from the process of this reaction ; and deduced the formula of the velocity of such reaction mentioned above with a calculated result of the apparent activation energy in this reaction by the curve showing the relationship among the consistency of starch, monomer and initiator and the velocity of the grafting copolymerization
摘要對澱粉接枝丙烯酸所得接枝共聚物及接枝側鏈物進行分離提純和分析測試,確定了其接枝效率並表徵了澱粉及其接枝物的形態結構;通過分別測定接枝共聚反應速率與澱粉、單體、引發劑濃度的關系曲線,確定了該接枝共聚反應的速率關系式;推算出了反應的表觀活化能。This paper is mainly concerned about how to purify the industrial products of the antioxidant d and bht, how to determine their purities, determining their purities and the purities need to be more than 99 %. in order to attain this objective, the recrystalizing method is used to purify antioxidant d and antioxidant bht. the methods of high performance liquid chromatography ( hplc ) is used to determine the chemical composition of the antioxidant d and bht, it is qualitative analysis
本論文是以防老劑d與bht工業品為主要原料制備防老劑d與bht標準物質,首先進行了防老劑d與bht的提純和熔點的測定試驗,並通過實驗確定了防老劑d與bht重結晶提純工藝;然後設計區域熔融裝置,擬定操作規程和技術條件,通過用區域熔融法提純重結晶后的防老劑d和bht產品滿足標準物質的純度要求。The quantity of each impure element is at ppt level, which offers the most superior reagent in purity on the market
每一不純元素的量均在ppt之等級,為市面上最高純度之試劑。Standard test method for p - phenylenediamine antidegradants - purity by high performance liquid chromatography
使用高效液相色譜的p -苯二胺抗降解劑純度的標準試驗方法General rule for test methods of highly purified reagents
高純度試劑試驗方法的總則The authors hold that the gas - collecting materials, the purity of the reagents used for the analysis and test, and the probable contamination in the popularization of this technique
認為集氣材料的純度和分析測試中的使用試劑的純度,以及在野外采氣作業與室內分擔地可能引起了污染是影響這一技術推廣的關鍵所在。Standard test method for purity of monomeric plasticizers by gas chromatography
用氣相色譜法分析增塑劑單體純凈度的標準試驗方法Standard test method forp - phenylenediamine antidegradants purity by gas chromatography
用氣相色譜法測試p -苯二胺抗降解劑純度的標準試驗方法Standard test methods for rubber chemical accelerator - purity by high performance liquid chromatography
用高性能液相色譜法對亞磺酰胺加速劑純度的標準試驗方法分享友人