電化學固結 的英文怎麼說
中文拼音 [diànhuàxuégùjiē]
電化學固結
英文
electro chemical induration-
Glucose biosensors were then constructed by these nanocomposites, and their electrochemical properties had been explored. secondly, the self - assembled nanocomposite was formed by mwnts and biopolymer, and was used to study the electrochemical properties of nadh. and finally, the modified electrode which was formed by immobilizing small molecular onto electrode surface, was used to detect dsdna in the solution
本論文首先,將多壁碳納米管( mwnts )與納米顆粒相結合,制備的納米復合材料用於構建葡萄糖生物傳感器,並研究了它的電化學性質;然後,將mwnts與生物聚合物自組裝制備的納米復合材料用於研究nadh的電化學性質;最後,本文還將小分子自組裝固定在電極表面,用於測定溶液中的dsdna 。Methods : the sartorius muscle was processed by conventional chemical fixation and cryofixation followed by freezing substitution
方法:蟾蜍縫匠肌經常規化學固定以及超低溫快速冷凍固定、冷凍置換后,透射電鏡進行超微結構觀察。Perovskite - type complex oxides of la1 - xsrxga1 - ymgyo3 compositions are characteristic of superior intermediate temperature oxide - ion conductivity and chemical stability, which are expected to be used in solid oxide fuel cells, sensors, electrocatalysis, membrane separators and membrane reactors. they have highly promising prospects in energy, metallurgy, chemical engineering and environmental protection, etc. in this dissertation, improved embeded sintering method has been employed to prepare la0. 8sr0. 2ga1 - ymgyo3 ( lsgm ) electrolyte, and the contributing factors to preparation, microstructure characteristics, conduction properties and thermology properties of lsgm electrolyte have been investigated
鈣鈦礦結構la _ ( 1 - x ) sr _ xga _ ( 1 - y ) mg _ yo _ 3復合氧化物具有優異的中溫離子導電特性和化學穩定性,作為固體電解質可用於固體氧化物燃料電池、傳感器、電催化、膜分離和膜反應器等,在能源、冶金、化工、環保等領域具有廣泛的應用前景。In order to improve its cycle performance and reduce capacity loss, we have synthesized series of lithium nickel manganese vanadate by using the moist chemical method in the reaction conditions of different temperature and calcination time. the structure characterization and element analysis tests are preformed by means of xrd, ir, raman and xps
為了改善其循環性能以及減少充放電過程中的容量損失,我們對其中的ni2 +進行部分替代,採用濕化學方法合成出了錳對鎳不同取代量的產物linil _ 、 mn萬04 ,並結合xrd 、 xps 、 ir和r田刀an圖譜對其固溶度及摻入其中的錳的價態進行研究。A. the preparation of sliding ink for plastic printing. b., widely used in ht e preparation of double components epoxy paint and epoxy adhesive, the curing matter own fine mechanical and electrochemical property ; it is also applied in the manufacture of low temp
B二聚酸與多元胺反應生成具有活性胺基的聚酰胺,廣泛應用於製造雙組份環氧油漆及環氧粘結劑,固化物具有良好的機械電化學等性能。The effects of the fabrication conditions on the crystal structure, grain size, micromorphology and electrochemical performance of these materials have been studied in depth. the reaction mechanism of the low - heating solid - state reaction method has also been investigated. in addition, a novel electrochemical method ( rpg method ) based on the concept of " ratio of potentio - galvano - charge capacity " has been for the first time developed to determine the diffusion coefficient of lithium - ion within insertion - host materials on the basis of the spherical diffusion model
本論文較系統地考察了低熱固相反應法合成鋰離子電池正極材料的可行性問題,研究了工藝條件對材料的晶體結構、晶粒尺寸、微觀形貌及電化學性能等的影響,探討了低熱固相反應的機理,並通過引進「恆壓-恆流充電容量比」的概念,給出了一種測定鋰離子嵌入脫出固相擴散系數的新方法。The lung tissue for immunohistochemitry and laser scanning confocal microscopy were fixed and embedded. the morphological alteration of pulmonary neuroendocrine cells which stain for calcitonin gene - related peptide ( cgrp ), serotonin ( s - ht ) and luteinizing hormone ( lh ) were studied. the results of these were dealed with computer image analysis and statistical treatment
肺組織取材后經固定、梯度酒精脫水、包埋、連續切片后,應用免疫組織化學方法、透射電鏡及激光掃描共聚焦技術觀察了降鈣素基因相關肽( cgrp ) 、五羥色胺( 5 - ht ) 、黃體生成素( lh )陽性細胞的隨齡變化,並對實驗結果進行了計算機圖像分析和統計學處理。So piezoelectric immunnosensors is gradually applied to some fields such as biochemical research, clinical analyze, environment and industry process assay. according to different method of immobilized antigens or antibodies, developed some new piezoelectric immunnosensors to determine proteins in consult serum
湖南大學分析化學碩士論文李丹200年6月本文結合壓電免疫傳感器抗體(抗原)固定化方法的不同,研製了一些新的壓電免疫傳感器用於參考血清中的一些蛋白的測定。( 3 ) volume shrinkage of composite decreases greatly with wpu increasing, even can arrive a negative number, but thermal stability is still good. ( 4 ) toughening mechanism is that : the formation of high molecular linear amino formate construct is the toughening reason ; hydroxyl - terminated pu - prepolymer and pf react to produce chemical bond effect which participate cure ; carboxyl - terminated pu - prepolymer and pf form semi - ipn which make toughened pf occur maximum
( 4 )通過紅外光譜對pf / pu共混物分子結構進行的定性分析、以及掃描電鏡對沖擊斷面形貌進行的分析,可證明聚氨酯預聚物增韌酚醛樹脂的機理是:兩個體系都是由於高分子量的線形氨基甲酸酯結構而增韌;端羥基pu與pf在共固化中產生化學鍵效應,參與pf的固化;而端羧基pu則與pf形成半互穿網路而增韌。The na2fepo4f cathode materials for sodium ion battery were prepared by solid state reaction and the influence of synthesizing temperature and morphology on the electrochemical performance of na2fepo4f powders in sodium ion batteries were systematically studied. the results indicate that na2fepo4f synthesized at 750 exhibited good electrochemical performance, whose first specific discharge capacity is 60mah / g, after 20 times cycling, the average specific discharge capacity is 51. 1mah / g
首先採用固相法制備了氟磷酸亞鐵鈉粉體,研究了不同煅燒溫度對合成材料顯微結構和電化學性能的影響,結果表明750下合成材料體現出較好的電化學性能,首次放電容量為60mah / g ,循環20次后,容量下降為51 . 1mah / g 。Piezoelectric sensing technique has been applied to many fields, including analytical chemistry, life science, environmental monitoring and surface sciences because of it ' s small size, high sensitivity, simplicity, low power consumption and broad sensing spectrum. piezoelectric immunosensors possess high selectivity provided by antibodies or antigens and sensitivity response directly to the mass change of proteins. immobilization technologies of biomolecules are of paramount importance in order to preserve their biological activity
壓電免疫傳感技術利用壓電晶體與抗原抗體特異性免疫反應結合的特徵,通常在壓電石英晶體表面先固定抗原(抗體) ,響應溶液中抗體(抗原)引起的質量、密度和粘度等性質的變化,它兼具有壓電質量響應的高靈敏性和生物化學反應的高特異性。The fitness of four negative electrode materials such as al, fe, zn, cd, and of six membranes materials : microfiber glass mat separator, polyethylene, polypropylene, polyvinyl chloride, vinylon, soapnated cellulose acetate, and of four current collects : carbon fiber ; nickel foam ; nickel foam sthongthened by iron wire net, punched silver grid in the super - iron alkaline batteries was comparatively studied. the influence of two storaged method ( with and without electrolyte ) and two impurities ( zno, fe ( oh ) 3 ) to the experiment cell ' s self - discharge nature was also comparatively studied. at last, the nature of discharge. structure and electrochemistry of experimental cell with k2feo4 as cathode active material prepared by three different methods : high temperature reaction, hypochlorite oxidizing and electrolysis, was comparative ly studied. we can conclude : i ) the open - circuit potential and the flat of work potential and the percent of capacity of k2feo4 till 1. 0v during the discharge at constant load of experimental cells decreased by the order of al / k2feo4, zn / k2feo4, cd / k2feo4, fe / k2feo4. as for the nature of charge - discharge cycle, cd / k2feo4 fe / k2feo4 zn / k2feo4. in water solute electrolyte, although al / k2feo4 can n ' t be used as storage battery, it have great potential as primary cell or storage cell from the aspect of its discharge capacity. discharge power
採用組裝實驗電池、 x -射線衍射( xrd )和循環伏安( cv )的方法,從實驗電池的放電特性、充放電循環特性、自放電特性,不同高鐵酸鹽的結構特性和電化學特性幾個方面,對4種金屬負極材料( al 、 fe 、 zn 、 cd ) 、 6種隔膜材料(復合玻璃纖維、幅射接枝聚乙烯、改性聚丙烯、聚氯乙烯、維尼綸無紡布、皂化再生纖維素) 、 4種集流體材料(泡沫鎳、以鐵網為加強層的泡沫鎳、切拉銀網、炭纖維編織網)在堿性高鐵電池中的適用性進行了比較研究;對2種雜質組分( zno 、 fe ( oh ) _ 3 )和2類不同貯存方式(干、濕)對實驗電池自放電特性的影響進行了比較研究;對3種方法(高溫固相反應、次氯酸鹽氧化、直流電解)所制k _ 2feo _ 4的實驗電池的放電特性、結構特性和電化學性能進行了比較研究。The present studies have proved that the most important factor which influences the performances of lithium metal anode in battery is the solid electrolyte interphase interface - film ( sei film ) on lithium anode. and how to make lithium metal anode have a sei film with favorable composition and stable configuration, or make the sei film have better stability, is the key to improve the electrochemistry performances of lithium metal anode in lithium secondary battery
已有的研究證明:影響金屬鋰負極在電池中性能的主要因素是其表面的固體電解質中間相界面膜( sei膜)的性能;如何使鋰金屬電極表面具有組成良好、結構穩定的sei膜,或者使鋰電極表面sei膜能夠更好的「穩定化」 ,是提高鋰二次電池中鋰金屬負極電化學性能的關鍵。The recent developments in normal spinel limn2o4 were reviewed, in the process of the solid state synthesis, we researched the effect of materials and synthesis temperature on crystal structure and electrochemical performance, which were characterized by dta - tg, sem, xrd as well as electrochemical performance testing. the structure, electrochemical performance and the correlations between them were all discussed in detail for these doped samples
本文在綜述國內外鋰離子電池尖晶石型材料limn _ 2o _ 4研究進展的基礎上,結合dta - tg 、 sem 、 xrd和電化學性能測試等手段,系統研究了固相法制備鋰離子電池正極材料摻鈷錳酸鋰合成原料、合成溫度對所得材料外觀形貌、晶體結構和電化學性能的影響。From the results of the experiment, we can see that simultaneity electrochemical polymerization of 3 - pyrrole - dna and 3 - [ 2, 5, 8, 11 - tetraoxa - tridecyl - 13 - ol ] - pyrrole was a new promising method for preparing dna chips because this method had such following advantages : first, the immobilization procedure can be controlled easily. second, with the progress of microelectronics, the miniaturization and integraterization of polypyrrole - based dna chip can be achieved in the future ; third, using an electrochemical active compound like the mb, the hybridization detection will be performed more easily
從以上實驗結果可看出,電化學聚吡咯方法制備dna晶元和傳統的方法相比具有下列優越性:首先,固定可通過電化學信號控制和完成,操作簡單易行;其次,微電子技術和電化學的進一步結合,可以提高晶元的集成程度,將dna晶元進一步向產業化方向推進;第三,通過應用電化學活性物質,有望建立無標記的dna晶元檢測技術,有利於減少環境污染、提高靈敏度、降低成本。For xlpe insulated power cable, either chemical method or physical method is employed to transform the molecular structure of pe from chain into three - dimensional network, i. e. thermoplastic pe is transformed into thermosetting xlpe. after cross - linking, the thermal and mechanical properties of pe have been greatly improved while its excellent electrical property are still retained
交聯聚乙烯絕緣電力電纜是採用化學方法或物理方法,使聚乙烯分子由線形分子結構轉變為三維網狀結構,由熱塑性的聚乙烯變成熱固性的交聯聚乙烯,從而提高了聚乙烯的耐老化性能、機械性能和耐環境能力,並保持了優良的電氣性能。In this work, layered lini1 - xalxo2 ( 0 < x 1 / 2 ) solid solution materials were successfully synthesized by current co - precipitation method in the air, and their preparation and properties were deeply and systematically explored. influences of different factors on the structure and properities of samples were studied, including li resources, different performs, li / m ( oh ) 2 molar ratio, calcining heat condition, the best synthesis technics were concluded : sintered for 16h at 700 from li source ( lithium nitrate ) : m ( oh ) 2 = 1. 05 : 1, ultrasonic vibration for dispersing and catalysing are best. lini0. 8al0. 2o2 exhibited a discharge capacity of 130. 7 mah ? g - 1 in the voltage range of 2. 8 ~ 4. 40v and at a specific current of 0. 2 c. a new co - precipitation method was proposed, it included ultrasonic for dispersing and catalysing, by dropping lioh to the aqueous solution of metal nitrates, hydroxides of metals were precipitated and the resulting solution was evaporated as received
採用傳統共沉澱工藝在空氣氣氛中成功地合成出了二元lini1 - xalxo2 ( 0 < x 1 / 2 )層狀固溶體系列,綜合考察了不同鋰源、預處理方式、鋰的配比量、焙燒溫度等條件對合成產物的結構和性能的影響,確定出了最佳合成工藝:以硝酸鋰為鋰源,超聲波作為分散動力源,鋰源與鎳鋁金屬鹽摩爾比為1 . 05 : 1 , 700下焙燒16h的lini0 . 8al0 . 2o2樣品電化學性能最佳,在2 . 8 ~ 4 . 40v之間, 0 . 2c的倍率放電可逆容量達130 . 7mah ? g - 1 。The dna electrochemical sensor was prepared by self - assembling the designed hepatitis b virus dna specific probe on the surface of au electrode together with hoechst 33258 as electro - active indicator
利用自組裝單分子膜法,將人工合成的乙肝病毒單鏈dna片斷作為特異性探針固定在金電極表面,結合電活性指示劑hoechst33258構成dna電化學傳感器。In this paper lifepo _ 4 powders were prepared via solid - state reactions mehtod that involve multiple steps at high temperatures. the effects of synthesis conditions on structure and electrochemical behavior of lifepo _ 4 were studied
採用高溫固相法制備lifepo _ 4 ,研究了合成條件對lifepo _ 4結構和電化學性能的影響,並嘗試了對材料進行摻雜改性。Doping of tio2 moo3 cro3 peo also improves the stability of sols, the performance of this electrochromic materials. when the optimum sintering treatment temperature is 200c, the ec layer has excellent electrochemistry performance and firmly integrated with glass substrate. doping of tio2 improves the stability of ceo2 and change the electrochemistry performance of sols markedly
本文研究了該全固態電致變色器件的顏色變化、響應時間、電化學性能、保存時間,並著重研究了電致變色層的循環次數、晶型結構、以及其前驅物的均勻性、穩定性和適宜的粘度。分享友人