熱顯微鏡學 的英文怎麼說
中文拼音 [rèxiǎnwéijìngxué]
熱顯微鏡學
英文
thermomicroscopy-
Based on the review, the main objectives of this work had been determined. the thermodynamic analysis indicated that corundum - mullite - gahnite multiphase materials can be synthesized. the investigation of x - ray diffraction ( xrd ) and scan electron microscope ( sem ) proved the validity of thermodynamics research
通過對al _ 2o _ 3 - sio _ 2 - zno體系相關反應熱力學的計算表明能夠合成出剛玉?莫來石?鋅鋁尖晶石復相材料， x ?射線衍射（ xrd ）和掃描電子顯微鏡（ sem ）的研究證實了熱力學計算的可靠性。The dependence of oxygen precipitation and induced - defects in heavily as - doped silicon on heat treatment process was studied by annealing and ig process, chemical etching, scanning electron micrograph ( sem ) and transmission electron microscopy ( tem ). a developed ig technique was suggested and the mechanism of the influence of as on oxygen precipitation formation in heavily as - doped silicon was discussed
本文通過化學腐蝕、光學顯微鏡、掃描電鏡（ sem ） 、透射電境（ tem ）等分析技術，對重摻砷硅單晶在單步退火工藝和內吸雜退火工藝中氧沉澱及誘生缺陷的形態，形核與熱處理溫度、時間的關系等進行了研究。The major performances of concrete and mortars, which are mixed with different quantities of expansion admixtures under the same mix proportions, are studied systematically and deeply in this work. sulphoaluminate mixed with a type of new expanding component by use of the composite methods are studied in the laboratory, and some achievements have been obtained. the service conditions, the characteristics and the shortcomings of expansion admixture in the concrete engineering are analyzed and summarized based on literatures, and the expanding mechanism of concrete is discussed
本文試圖從膨脹劑不同摻量研究其對混凝土和砂漿主要性能的影響，進行了一系列宏觀力學性能試驗研究；利用差熱分析（ dta ） 、掃描電子顯微鏡（ sem ）等分析手段對鈣礬石等水化產物的結晶和生成量、形貌特徵進行微觀分析；並採用復合方法摻加新型膨脹組分對硫鋁酸鹽類膨脹劑（ uea ）進行了改性試驗研究，根據多因素模糊綜合評價方法就各類膨脹劑的主要性能進行綜合評價，得出摻加新型膨脹組分pt的膨脹劑性能較優，取得了明顯的效果。Microstructure of the composite layer was analyzed with help of optical microscope, scanning electronic microscope ( sem ), electronic probe microanalysis ( epma ) and x - ray diffraction ( xrd ). the compacting of the billet and the forming mechanism of the carbide reinforcement were studied based on thermodynamics and kinetics of reaction, sintering theory and the result of dta. at the same time, the wear - resistance of the composite layer was studied under condition of dry sliding friction
利用光學顯微鏡、掃描電子顯微鏡、電子探針以及x -射線衍射儀，分析了表面復合層的基體組織結構；運用反應熱力學、動力學、粉末燒結理論和燃燒合成理論，結合差熱分析結果，探討了表面復合層壓坯的燒結緻密化原理和碳化物增強相的形成機理；利用坯塊在真空燒結爐不同溫度下的燒結出來的顯微組織分析，模擬出坯塊的燒結過程中的化學反應過程。Scanning electron microscope ( sem ) and energy dispersive spectrum ( eds ) have been used to observe the coating surface and analyze the composition
通過sem 、光學顯微鏡觀察鍍層表觀形貌及其熱振試驗對鍍層性能進行了表徵。This text completely and systematically studies the status and the development of the pyrolysis and the fluidization of biomass, which distill the bio - oil in the domestic and international area, as well as the existing problems. this thesis primarily include following aspects : ( l ), by experimenting and measuring the energy ( heat value ) and the content of c, h, n chemical element of right 20 kinds of common biomass, on the base of the experimental result, and respectively established the biomass energy predict experiment formula with the element of h and c is from change, and passed the ro. os examination, which provides the basis and convenience for flash pyrolysis fluidization device energy to convert the rate to compute with biomass energy utilization calculation ; ( 2 ), proceeded the tg and dtg experimentation equal velocity ( 10 ? / min, 20 ? / min, 40 ? / min, 60 ? / min ) heating and constant temperature heating by studying on eight kinds of biomass samples, according to the experimental data and arrhenius formula, we established the dynamics model of pyrolysis of, then, using the goast - redfern and p function, we also solved the dynamics parameters and analyze out every kind of biomass ' s frequency factor and parameters of activation energy, and established the every kind of dynamics model of pyrolysis of biomass, all of these provide the theories and basis to make sure the reactor ' s flash pyrolysis work temperature scope design and the describing of pyrolysis reactor dynamics ; ( 3 ), in order to study and ascertain the process of heat completely getting to pyrolysis time of varied size biomass particles, we observed and measured the ratio of length and diameter ( l / d ) with the varied biomass through electron microscope, we concluded the l / d ratios usually is from 5. 0 to 6. 0, the average is 5. 3 ; ( 4 ), we studied the process of biomass transiting and the theory of complete pyrolysis time with the theory of complicated heat field, we got the time ( t ) of the varied size biomass particles arriving to complete pyrolysis, and we knew that the complete pyrolysis time and the time which get to the biggest production ratio are identical, all of these studies provide the theory base for design and forecasting the flash pyrolysis reactor solid state resort time ; ( 5 ), according to the above experiment result, synthesize to make use of the engineering the mechanics, engineering the material, machine the design to learn the principle, deduce, establish the theory of rotation cone flash pyrolysis reactor material resort time ( t ) and reasonable rotation velocity ( or frequency ) relation theory ; and ( 6 ), we gave the reactor ' s smallest cone angle certain, reactor cone wall strength design theory, the reactor production ability theory, the power design method and the critical rotation velocity theory
本文較全面、系統地綜述了國內外生物質熱解液化制取生物燃油技術研究發展現狀及存在的問題，主要研究內容有： （ 1 ）實驗、測定了20種常見生物質的能量（發熱量）和c 、 h 、 n元素含量，根據實驗結果分別建立了以h和c為自變量的生物質能量預測經驗公式，並通過r _ （ 0 . 05 ）檢驗；為閃速熱解液化裝置能量轉化率計算和生物質能量利用率計算提供了依據和方便； （ 2 ）選擇了8種生物質試樣作了等加熱速率（ 10 min 、 20 min 、 40 min 、 60 min ）和恆溫加熱的tg和dtg實驗，根據實驗數據和阿倫尼烏斯公式建立了生物質熱解反應動力學微分方程，並採用goast - redfem積分法和p函數對其動力學參數進行了求解，解析出各種生物質的頻率因子和活化能參數，進而建立了各種生物質的熱解動力學模型，為科學確定反應器的閃速熱解工作溫度范圍及熱解反應動力學描述，提供了理論和依據； （ 3 ）為研究和確定不同尺度的生物質顆粒中心達到全熱解的時間，在體視顯微鏡下對不同粒度的生物質顆粒的長徑比進行了實驗觀察和測定，得出生物質的長徑比（ l d ）一般在5 . 0 6 . 0之間，平均為5 . 3的結果； （ 4 ）採用復雜溫度場傳熱學理論對生物質傳熱過程及充分熱解時間理論進行了研究，解析推導出了不同尺寸生物質顆粒中心溫度達到充分熱解溫度的時間（ t ） ，得出了理論推導的充分熱解時間與最大產油率的熱解時間相一致的結果，為閃速熱解反應器固相滯留時間設計和預測提供了理論依據； （ 5 ）根據上述實驗結果，綜合運用工程力學、工程材料、機械設計學原理，推導、建立了轉錐式閃速熱解反應器物料滯留時間（ ）與轉速（或頻率）合理匹配理論； （ 6 ）提出了轉錐式閃速熱解反應器的最小錐角設計、錐壁強度設計、生產能力設計理論和功率計算方法及臨界轉速理論等。The influence of different technological conditions including ph. mass ratio of gelation, the time of gelation, as well as the hardening time on yields of microcapsulation the efficiency of encapsulation were studied respectively. the microencapsulation condition were also optimized
採用光學顯微鏡、 tem 、 sem 、激光粒度分析儀研究了微膠囊的表面形態、包覆效果和粒徑分佈；採用tg和dsc研究了微膠囊的熱穩定性和儲熱調溫效果。Using the microwave selective heating property for materials, by setup equivalent equation, and first time inducing the electromagnetic field perturbation theory to the design of heating materials for substrate in mpcvd, three temperature distribution modes were established, including temperature distribution comprehensive mode of inhomogeneous plasma, temperature distribution composite mode of composite substrate materials, temperature distribution perturbation mode of composite materials, which ii provided an whole new technology route to the design of substrate heating system in mpcvd and guided the preparation of heating materials for substrate. and then the heating materials for substrate were designed and optimized to obtain large area homogeneous temperature distribution even larger than substrate holder ' s diameter. as an important part, this thesis researched the nucleation and growth of diamond films in mpcvd, systematically researched the effects of substrate pretreatment, methane concentration, deposition pressure and substrate temperature etc experimental technologic parameters on diamond films " quality on ( 100 ) single crystal silicon substrate in the process of mpcvd, characterized the films qualities in laser raman spectra ( raman ), x - ray diffraction ( xrd ), scanning electron microscopy ( sem ), infrared transmission spectra ( ir ), atomic force microscopy ( afm ), determined the optimum parameters for mpcvd high quality diamond in the mpcvd - 4 mode system
該系統可通過沉積參數的精確控制，以控制沉積過程，減少金剛石膜生長過程中的缺陷，並採用光纖光譜儀檢測分析等離子體的可見光光譜以監測微波等離體化學氣相沉積過程；利用微波對材料的選擇加熱特性，通過構造等效方程，並首次將電磁場攝動理論引入到mpcvd的基片加熱材料的設計中，建立了非均勻等離子體溫度場綜合模型、復合介質基片材料的復合溫度場模型及復合介質材料溫度場攝動模型，為mpcvd的基片加熱系統設計提供了一條全新的技術路線以指導基片加熱材料的制備，並對基片加熱材料進行了設計和優選，以獲取大面積均勻的溫度場區，甚至獲得大於基片臺尺寸的均勻溫度區；作為研究重點之一，開展了微波等離體化學氣相沉積金剛石的成核與生長研究，系統地研究了在（ 100 ）單晶硅基片上mpcvd沉積金剛石膜的實驗過程中，基片預處理、甲烷濃度、沉積氣壓、基體溫度等不同實驗工藝參數對金剛石薄膜質量的影響，分別用raman光譜、 x射線衍射（ xrd ） 、掃描電鏡（ sem ） 、紅外透射光譜（ ir ） 、原子力顯微鏡（ afm ）對薄膜進行了表徵，確立了該系統上mpcvd金剛石膜的最佳的實驗工藝參數。Ir - ta - ti metal oxide coated titanium anodes of variable composition were prepared by thermal decomposition. their micro morphorogies and electrochemical properties were characterized by scanning electron microscope, open circuit potential, cyclic voltammetry, consumption rate measurements and accelerated life test. the sem results indicated that all coatings were of a porous and cracked - mud microstructure influenced greatly by the composition of coatings. the electrochemical measurements showed that the ir - ta - ti ternary oxide - coated anodes exhibited excellent electrochemical activity and electrochemical stability in both acidic media and seawater which were affected by the composition and microstructure of the coatings. owing to good corrosion resistance and low consumption rate in seawater, metal oxde coated anodes belong to insoluble material, and can be potentially applid in impressed current cathodic protection systems as an anode
採用熱分解方法在鈦基體上制備銥鉭鈦金屬氧化物陽極，用掃描電鏡對陽極塗層顯微形貌進行分析，通過強化電解壽命試驗、開路電位測試、消耗率試驗及循環伏安曲線研究了金屬氧化物陽極的電化學性能. sem分析結果表明銥鉭鈦金屬氧化物陽極塗層呈現多孔多裂紋形貌結構.隨陽極塗層組成不同，塗層顯微形貌表現出很大差異，這種差異直接影響陽極電化學性能.電化學性能試驗結果表明銥鉭鈦金屬氧化物陽極在酸性介質和海水中具有良好的電化學穩定性和電化學活性.此外，銥鉭鈦金屬氧化物陽極在海水中的消耗率很低，屬于不溶性的陽極材料，作為外加電流陰極保護用輔助陽極具有廣泛的應用前景Catalysts were prepared by impregnation reduction, thermal reduction, advanced thermal reduction and sol - gel methods from these metals. electrochemistry measurements, xrd, tem were used to test these catalysts. the results showed that these metals have some electrocatalysis activities towards hydrogen oxidation reaction
本文選擇了w 、 mo 、 co等金屬，採用浸漬還原法、熱還原法、改進的熱還原法以及溶膠凝膠法分別制備了這幾種金屬的碳載催化劑，對制備出的非貴金屬催化劑進行了電化學測試、 x -射線衍射（ x - raydiffraction ， xrd ） 、透射電子顯微鏡（ transmissionelectronmicroscopy ， tem ）等測試，研究結果表明:這些非貴金屬在硫酸體系中對氫氣的氧化反應均有一定的催化活性。The principles of differential scanning calorimetry, electron microscope, nuclear magnetic resonance and x - ray were introduced in this paper together with their applications in oil quality control, development direction of investigation on oil quality control was also forecasted here
摘要介紹了現代物理化學方法（差示掃描量熱法、電子顯微鏡、核磁共振法、 x -射線衍射法）的原理及其在油脂質量控制中的應用，並預側了油脂質量控制研究的發展方向。The synthesis process of swnts by catalytic chemical vapor deposition ( ccvd ) was investigated and the product was characterized by transmission electron microscopy ( tem ), thermo - gravimetric analysis ( tga ) and raman scattering spectra and so on in this thesis
本文研究了單壁納米碳管的化學氣相沉積法制備工藝，並運用透射電子顯微鏡（ tem ） 、熱重分析（ tga ）與拉曼（ raman ）光譜等分析手段，對產物及催化劑進行了表徵。According to the significant improvement in properties of ions and particles doped perovskite, tb and cnt doped pt materials were prepared, and the properties studied. tb and cnt doped pt powders and films were successfully prepared by sol - gel method. by differential thermal analysis ( dta ), scanning electron microscopy ( sem ), transmission electron microscopy ( tem ), x - ray diffraction ( xrd ), fluorescent analysis and dielectric constant analysis, the morphology and phase transformation, crystalline properties, fluorescent properties and dielectric properties of the materials were studied
本研究中採用溶膠凝膠法制備了具有優良結晶性能的稀土離子tb及納米碳管摻雜的鈦酸鉛（ pt ）超細粉末和（ 100 ）取向生長的薄膜，並利用差熱分析、掃描電子顯微鏡、透射電子顯微鏡、 x射線衍射、熒光分析和介電常數等多種分析測試手段對摻雜后的pt薄膜及超細粉末的相結構、光學性能、結晶性能以及介電常數等進行了研究。In this article, molybdenum wire multi - doped with la2o3 and k, al, si, molybdenum wire doped with k, al, si and molybdenum wire doped with la2o3 or y2o3 are analyzed by dsc, hot - draw, sem, optical microscope, micro - hardness, x - ray and tem. it is found that multi - doped molybdenum wire is better at elevating the recrystallization temperature and improving the micro - structure and mechanic properties after recrystallization than molybdenum wire doped with k, al, si
本文通過差熱分析、熱模擬、掃描電鏡、金相顯微鏡、顯微硬度、 x射線衍射和透射電鏡等實驗手段對復合摻雜k 、 al 、 si和稀土氧化物的鉬絲、單摻雜k 、 al 、 si的鉬絲以及單摻雜稀土氧化物的鉬絲的再結晶溫度、高溫下的綜合力學性能和組織形貌進行了綜合對比分析。The resulting polymers were characterized by " h - nmr, ir, dsc, pom, gel permention chromatography ( gpc ). the relations between structures and properties were studied systemtically. the influences of the lateral rod content on the polymers " solubility and the stability of liquid crystalline states and chemical structures were discussed in detail
經過凝膠色譜（ gpc ） 、偏光顯微鏡（ pom ） 、差示掃描量熱（ dsc ） 、 ~ 1h - nmr和ir對聚合物的化學結構和液晶性進行了表徵，系統研究了聚合物結構和性質之間的關系。The configuration and microstructure of production, the effect of heating temperature and chemistry match ratio on reaction and production, the effect of calcining temperature and time on the changes of production crystal were studied by xrd, tem, dta and microscope
本文通過xrd 、 tem 、差熱分析、金相顯微鏡等手段對所制備材料的結構、組織形貌、點火溫度和化學配比對反應現象和反應產物的影響、煅燒溫度和煅燒時間對產物晶型轉變的影響等方面進行了分析研究。6013 aluminum alloys containing different main alloying elements minor alloying elements were designed and prepared by ingot - metallurgy processing. the tesile mechanical and aging properties of the studied alloys were tested ; the microstructure of those alloys were observed and analyzed using optical microscope ; the influence of main alloying element mg, si, minor alloying elements mn, cu and homogenization process on the structure and property of studied alloys were studied
採用鑄錠冶金方法，設計並制備了不同合金元素含量的6013鋁合金，將鑄錠熱加工以後，測試了合金的拉伸力學性能和時效性能，採用金相顯微鏡觀察分析了合金的顯微組織結構，研究了合金中主合金元素mg 、 si ，微量元素mn 、 cu添加量、均勻化溫度和時間對合金組織和性能的影響。分享友人