熱顯微鏡法 的英文怎麼說
中文拼音 [rèxiǎnwéijìngfǎ]
熱顯微鏡法
英文
thermomicroscopy-
By the methods of epn ( electronic probing needle ) 、 sem and xed, the formation mechanisms of the wear - resistant composite layer are studied, the results indicated that, molten iron has infiltrated into the alloying layer under capillary action. this caused ht powder, whose fusion point is low relatively, to be surperheated and formed a surface composite layer
利用電子顯微鏡及x射線衍射等試驗方法，研究了復合層形成機理，研究表明，復合層是在毛細力作用下，鐵液被吸入合金層中，致使低熔點ht粉過熱熔化而形成的，並與母材是冶金結合。The composite roll of high speed steel has the synthetical life of over ten times more than traditional high cr cast iron roll. now the research and production of the high speed steel for roll are very drastic. in this thesis, the microstructure, heat treatment and performance of high speed steel fe - 2 % c - 4 % v - 4 % mo - 5 % cr - x % w ( wt ) are studied systematically by using metallograph, method of lattice, xrd, sem, eds and hardness
本文利用金相法（包括黑白金相和彩色金相） 、 x射線衍射（ xrd ） 、掃描電子顯微鏡（ sem ） 、能譜（ eds ）及洛氏硬度分析儀等手段，對復合軋輥用高速鋼fe - 2 c - 4 v - 4 mo - 5 cr - x w （其它部分如未作特殊註明均為質量分數）合金系的顯微組織、熱處理工藝及性能進行了系統地分析。The major performances of concrete and mortars, which are mixed with different quantities of expansion admixtures under the same mix proportions, are studied systematically and deeply in this work. sulphoaluminate mixed with a type of new expanding component by use of the composite methods are studied in the laboratory, and some achievements have been obtained. the service conditions, the characteristics and the shortcomings of expansion admixture in the concrete engineering are analyzed and summarized based on literatures, and the expanding mechanism of concrete is discussed
本文試圖從膨脹劑不同摻量研究其對混凝土和砂漿主要性能的影響，進行了一系列宏觀力學性能試驗研究；利用差熱分析（ dta ） 、掃描電子顯微鏡（ sem ）等分析手段對鈣礬石等水化產物的結晶和生成量、形貌特徵進行微觀分析；並採用復合方法摻加新型膨脹組分對硫鋁酸鹽類膨脹劑（ uea ）進行了改性試驗研究，根據多因素模糊綜合評價方法就各類膨脹劑的主要性能進行綜合評價，得出摻加新型膨脹組分pt的膨脹劑性能較優，取得了明顯的效果。Surface microtopography, representation and tracer of microscale vortex dislocation of hydrothermal synthetic sapphires and natural beryls are studied by using atomic force micro - scope and interference microscope
摘要採用原子力顯微鏡、干涉顯微鏡對水熱法合成藍寶石和天然綠柱石等寶石的表面微形貌進行了研究。Furthermore, the growth and the study of self - organized quantum dots structures become more and more important recently, and the application of self - organization technique become wider and wider in this thesis, we address the theory of film growth and the growth technique firstly more, the ways and characteristics of surface detection are prescribed we mainly report the growth process, results and discuss of self - organized quantum dots structures in the a12o3 substrates by s - k mode using ecr - mocvd, in the espd - u device the growth art of ain epilayer which is the preliminary foundation of self - organized gan / ain quantum dots structures, including the substrate cleaning, nitridation, the growth of buffer and the growth of gan and ain epilayer, is discussed we deliberately compare the test result of rheed xrd and afm and achieved the optimalized condition of ain at last we have successfully realized the growth of ain which is much smooth and better crystal quality moreover, we grow the self - organized gan / ain quantum dots structure in s - k mode because the limits of the heater temperature, we can not grow the atom - smooth epilayer of ain until now so we could not grow better quantum dots which have small diameter and big density but the self - organized quantum dots structures with better quality will be realized successfully if the substrate temperature is increased the thesis study belong to my tutor subject of national nature science foundation ( 69976008 )
本論文主要論述了在espd - u裝置上，採用電子迴旋共振等離子體增強mocvd （ ecr - pamocvd ）方法，在藍寶石襯底上通過s - k模式自組裝生長gan aln量子點結構的生長工藝、結果及討論。而重點分析了自組裝生長量子點之前的aln外延層生長工藝，包括襯底清洗、氮化、緩沖層的生長和gan 、 aln外延層的生長；通過高能電子衍射、 x射線衍射和原子力顯微鏡測試，並且對這些測試結果進行了詳細的比較研究，得出了較優化的工藝條件，生長出了晶質較好、表面較平整的aln外延層；進而採用s - k模式自組裝生長了gan aln量子點結構。由於實驗裝置加熱爐溫度的限制，我們沒有能夠生長出原子級平滑的aln外延層表面，因而沒能夠生長出密度比較大和直徑比較小的量子點。Salt alginate fiber was prepared by means of wet spinning, the structure and properties of the fibers were studied by differential thermal analysis, infrared and scanning electron microscopy
摘要採用溶液紡絲的方法制備了海藻酸鹽纖維，藉助熱分析、紅外分析及掃描電子顯微鏡等對纖維結構與性能進行了研究。The pretreatment, effect of bath compositions and operation conditions such as temperature, currenty and time on compactness of the zinc and cu / ni / cr coatings have been investigated. the relationship of operation conditions to thickness of the coatings was studied by weight method. the specimens have been pickled in nacl or sulfate acid solution to evaluate the porosity of the coating
研究了鎂合金電鍍前處理工藝，電鍍鋅、電鍍銅/鎳/鉻工藝配方及其施鍍溫度、電流密度和時間對鍍層緻密性的影響;採用稱重法研究施鍍工藝與鍍層厚度的關系，利用nacl溶液和硫酸溶液浸泡試樣來考察鍍層孔隙率，採用劃痕試驗和熱震試驗檢驗鍍層的結合力，採用金相顯微鏡和掃描電子顯微鏡觀察鍍層表面形貌。This text completely and systematically studies the status and the development of the pyrolysis and the fluidization of biomass, which distill the bio - oil in the domestic and international area, as well as the existing problems. this thesis primarily include following aspects : ( l ), by experimenting and measuring the energy ( heat value ) and the content of c, h, n chemical element of right 20 kinds of common biomass, on the base of the experimental result, and respectively established the biomass energy predict experiment formula with the element of h and c is from change, and passed the ro. os examination, which provides the basis and convenience for flash pyrolysis fluidization device energy to convert the rate to compute with biomass energy utilization calculation ; ( 2 ), proceeded the tg and dtg experimentation equal velocity ( 10 ? / min, 20 ? / min, 40 ? / min, 60 ? / min ) heating and constant temperature heating by studying on eight kinds of biomass samples, according to the experimental data and arrhenius formula, we established the dynamics model of pyrolysis of, then, using the goast - redfern and p function, we also solved the dynamics parameters and analyze out every kind of biomass ' s frequency factor and parameters of activation energy, and established the every kind of dynamics model of pyrolysis of biomass, all of these provide the theories and basis to make sure the reactor ' s flash pyrolysis work temperature scope design and the describing of pyrolysis reactor dynamics ; ( 3 ), in order to study and ascertain the process of heat completely getting to pyrolysis time of varied size biomass particles, we observed and measured the ratio of length and diameter ( l / d ) with the varied biomass through electron microscope, we concluded the l / d ratios usually is from 5. 0 to 6. 0, the average is 5. 3 ; ( 4 ), we studied the process of biomass transiting and the theory of complete pyrolysis time with the theory of complicated heat field, we got the time ( t ) of the varied size biomass particles arriving to complete pyrolysis, and we knew that the complete pyrolysis time and the time which get to the biggest production ratio are identical, all of these studies provide the theory base for design and forecasting the flash pyrolysis reactor solid state resort time ; ( 5 ), according to the above experiment result, synthesize to make use of the engineering the mechanics, engineering the material, machine the design to learn the principle, deduce, establish the theory of rotation cone flash pyrolysis reactor material resort time ( t ) and reasonable rotation velocity ( or frequency ) relation theory ; and ( 6 ), we gave the reactor ' s smallest cone angle certain, reactor cone wall strength design theory, the reactor production ability theory, the power design method and the critical rotation velocity theory
本文較全面、系統地綜述了國內外生物質熱解液化制取生物燃油技術研究發展現狀及存在的問題，主要研究內容有： （ 1 ）實驗、測定了20種常見生物質的能量（發熱量）和c 、 h 、 n元素含量，根據實驗結果分別建立了以h和c為自變量的生物質能量預測經驗公式，並通過r _ （ 0 . 05 ）檢驗；為閃速熱解液化裝置能量轉化率計算和生物質能量利用率計算提供了依據和方便； （ 2 ）選擇了8種生物質試樣作了等加熱速率（ 10 min 、 20 min 、 40 min 、 60 min ）和恆溫加熱的tg和dtg實驗，根據實驗數據和阿倫尼烏斯公式建立了生物質熱解反應動力學微分方程，並採用goast - redfem積分法和p函數對其動力學參數進行了求解，解析出各種生物質的頻率因子和活化能參數，進而建立了各種生物質的熱解動力學模型，為科學確定反應器的閃速熱解工作溫度范圍及熱解反應動力學描述，提供了理論和依據； （ 3 ）為研究和確定不同尺度的生物質顆粒中心達到全熱解的時間，在體視顯微鏡下對不同粒度的生物質顆粒的長徑比進行了實驗觀察和測定，得出生物質的長徑比（ l d ）一般在5 . 0 6 . 0之間，平均為5 . 3的結果； （ 4 ）採用復雜溫度場傳熱學理論對生物質傳熱過程及充分熱解時間理論進行了研究，解析推導出了不同尺寸生物質顆粒中心溫度達到充分熱解溫度的時間（ t ） ，得出了理論推導的充分熱解時間與最大產油率的熱解時間相一致的結果，為閃速熱解反應器固相滯留時間設計和預測提供了理論依據； （ 5 ）根據上述實驗結果，綜合運用工程力學、工程材料、機械設計學原理，推導、建立了轉錐式閃速熱解反應器物料滯留時間（ ）與轉速（或頻率）合理匹配理論； （ 6 ）提出了轉錐式閃速熱解反應器的最小錐角設計、錐壁強度設計、生產能力設計理論和功率計算方法及臨界轉速理論等。The structural characterization of v _ 2o _ 5 compounds were measured bymeans of differential thermoanalysis ( dta ) and thermogravimetry ( tg ), scanning electron microscopy ( sem ), and x - ray diffraction ( xrd ). the testsreveale that materials which were prepared by sol - gel ( inorganic sol gel andmelting - coling ) showed that the amorphous structure, and the interlayer spacingenlarge a lot than that of crystalline v _ 2o _ 5
採用熱重與差熱（ tg - dta ） ，掃描電子顯微鏡（ sem ） ， x射線衍射（ xrd ）等測試手段對材料的結構性能進行表徵，結果顯示兩種溶膠-凝膠法（無機溶膠凝膠法和熔融淬冷法）制備的v _ 2o _ 5材料均為無定型結構，其層面間距均比晶體v _ 2o _ 5成倍增大。Ir - ta - ti metal oxide coated titanium anodes of variable composition were prepared by thermal decomposition. their micro morphorogies and electrochemical properties were characterized by scanning electron microscope, open circuit potential, cyclic voltammetry, consumption rate measurements and accelerated life test. the sem results indicated that all coatings were of a porous and cracked - mud microstructure influenced greatly by the composition of coatings. the electrochemical measurements showed that the ir - ta - ti ternary oxide - coated anodes exhibited excellent electrochemical activity and electrochemical stability in both acidic media and seawater which were affected by the composition and microstructure of the coatings. owing to good corrosion resistance and low consumption rate in seawater, metal oxde coated anodes belong to insoluble material, and can be potentially applid in impressed current cathodic protection systems as an anode
採用熱分解方法在鈦基體上制備銥鉭鈦金屬氧化物陽極，用掃描電鏡對陽極塗層顯微形貌進行分析，通過強化電解壽命試驗、開路電位測試、消耗率試驗及循環伏安曲線研究了金屬氧化物陽極的電化學性能. sem分析結果表明銥鉭鈦金屬氧化物陽極塗層呈現多孔多裂紋形貌結構.隨陽極塗層組成不同，塗層顯微形貌表現出很大差異，這種差異直接影響陽極電化學性能.電化學性能試驗結果表明銥鉭鈦金屬氧化物陽極在酸性介質和海水中具有良好的電化學穩定性和電化學活性.此外，銥鉭鈦金屬氧化物陽極在海水中的消耗率很低，屬于不溶性的陽極材料，作為外加電流陰極保護用輔助陽極具有廣泛的應用前景Catalysts were prepared by impregnation reduction, thermal reduction, advanced thermal reduction and sol - gel methods from these metals. electrochemistry measurements, xrd, tem were used to test these catalysts. the results showed that these metals have some electrocatalysis activities towards hydrogen oxidation reaction
本文選擇了w 、 mo 、 co等金屬，採用浸漬還原法、熱還原法、改進的熱還原法以及溶膠凝膠法分別制備了這幾種金屬的碳載催化劑，對制備出的非貴金屬催化劑進行了電化學測試、 x -射線衍射（ x - raydiffraction ， xrd ） 、透射電子顯微鏡（ transmissionelectronmicroscopy ， tem ）等測試，研究結果表明:這些非貴金屬在硫酸體系中對氫氣的氧化反應均有一定的催化活性。The principles of differential scanning calorimetry, electron microscope, nuclear magnetic resonance and x - ray were introduced in this paper together with their applications in oil quality control, development direction of investigation on oil quality control was also forecasted here
摘要介紹了現代物理化學方法（差示掃描量熱法、電子顯微鏡、核磁共振法、 x -射線衍射法）的原理及其在油脂質量控制中的應用，並預側了油脂質量控制研究的發展方向。The performance of high and low temperature was improved simultaneity because the materials of modified asphalt had structure of the undee samdwich. the modified asphalt was characterized by element analysis, tem, xrd, tg and ft - ir. we discussed the possible mechanism of the modification
另外，還採用了透射電子顯微鏡（ tem ） 、 x射線衍射（ xrd ） 、熱重摘要分析（ tg ） 、紅外光譜分析（ ft - ir ）等分析方法對改性瀝青進行了表徵，探討了可能的改性機理。Amino acid molecules imprinted polymeric composite microspheres with magnetic susceptibility ( ms - smips ) were prepared by suspension polymerization ( sp ) and inverse emulsion - suspension polymerization ( iesp ), respectively. protein molecules imprinted soft - wet gel composite microspheres with magnetic susceptibility ( ms - pigms ) were prepared by inverse suspension polymerization ( isp ) and seeded inverse suspension polymerization ( sisp ), respectively. the resulting ms - smips and ms - pigms were characterized by scanning electron microscope ( sem ), thermogravimetric analyzer ( tg ), vibrating sample magnetometer ( vsm ), infrared spectrum ( ftir ), high performance liquid chromatography ( hplc ), and so on
分別採用懸浮聚合法和反相乳液?懸浮聚合法制備了氨基酸分子印跡聚合物磁性復合微球（ ms - smips ） ；分別採用反相懸浮聚合法和種子反相懸浮聚合法制備了蛋白質分子印跡磁性軟濕凝膠復合微球（ ms - pigms ） ；用掃描電子顯微鏡、熱重分析儀、振動樣品磁強計、紅外光譜、高效液相色譜等對所制備的ms - smips和ms - pigms進行了表徵。The synthesis process of swnts by catalytic chemical vapor deposition ( ccvd ) was investigated and the product was characterized by transmission electron microscopy ( tem ), thermo - gravimetric analysis ( tga ) and raman scattering spectra and so on in this thesis
本文研究了單壁納米碳管的化學氣相沉積法制備工藝，並運用透射電子顯微鏡（ tem ） 、熱重分析（ tga ）與拉曼（ raman ）光譜等分析手段，對產物及催化劑進行了表徵。According to the significant improvement in properties of ions and particles doped perovskite, tb and cnt doped pt materials were prepared, and the properties studied. tb and cnt doped pt powders and films were successfully prepared by sol - gel method. by differential thermal analysis ( dta ), scanning electron microscopy ( sem ), transmission electron microscopy ( tem ), x - ray diffraction ( xrd ), fluorescent analysis and dielectric constant analysis, the morphology and phase transformation, crystalline properties, fluorescent properties and dielectric properties of the materials were studied
本研究中採用溶膠凝膠法制備了具有優良結晶性能的稀土離子tb及納米碳管摻雜的鈦酸鉛（ pt ）超細粉末和（ 100 ）取向生長的薄膜，並利用差熱分析、掃描電子顯微鏡、透射電子顯微鏡、 x射線衍射、熒光分析和介電常數等多種分析測試手段對摻雜后的pt薄膜及超細粉末的相結構、光學性能、結晶性能以及介電常數等進行了研究。The modified asphalt may be looked upon materials for highway road. the sea and island structure which the island lied in the sea and the sea lied in the island of the modified asphalt was characterized by sem. the modified asphalt was characterized by element analysis, tem, afm, gpc, tg and ft - ir
通過掃描電子顯微鏡（ sem ）分析表明改性后瀝青呈島中有海、海中有島的海島結構；另外，還採用了元素分析、透射電子顯微鏡（ tem ） 、原子力顯微鏡（ afm ） 、凝膠色譜（ gpc ） 、熱重分析（ tg ） 、紅外光譜分析（ ft - ir ）等分析方法對改性瀝青進行了表徵，探討了可能的改性機理。6013 aluminum alloys containing different main alloying elements minor alloying elements were designed and prepared by ingot - metallurgy processing. the tesile mechanical and aging properties of the studied alloys were tested ; the microstructure of those alloys were observed and analyzed using optical microscope ; the influence of main alloying element mg, si, minor alloying elements mn, cu and homogenization process on the structure and property of studied alloys were studied
採用鑄錠冶金方法，設計並制備了不同合金元素含量的6013鋁合金，將鑄錠熱加工以後，測試了合金的拉伸力學性能和時效性能，採用金相顯微鏡觀察分析了合金的顯微組織結構，研究了合金中主合金元素mg 、 si ，微量元素mn 、 cu添加量、均勻化溫度和時間對合金組織和性能的影響。分享友人