熱液合成法 的英文怎麼說
中文拼音 [rèyègěchéngfǎ]
熱液合成法
英文
hydrothermal synthesis-
By the methods of epn ( electronic probing needle ) 、 sem and xed, the formation mechanisms of the wear - resistant composite layer are studied, the results indicated that, molten iron has infiltrated into the alloying layer under capillary action. this caused ht powder, whose fusion point is low relatively, to be surperheated and formed a surface composite layer
利用電子顯微鏡及x射線衍射等試驗方法，研究了復合層形成機理，研究表明，復合層是在毛細力作用下，鐵液被吸入合金層中，致使低熔點ht粉過熱熔化而形成的，並與母材是冶金結合。By physiognomy feature, it could be divided into three types of thermal structure : positive dome model, negative collapse model and border dome core collapse model. based on the depth degree or magma - thermal influenced, it could be divided into five types of thermal structure : ( ancient ) geothermal anomaly focus region model, superficial volcano eruption hydro - thermalism and hypabyssal intrusive model, thermal anticline ( thermal dome ) model, mid - deep intrusive model, deep mantle ( crust ) thermal plume model ; and put forward a perfect model of the thermal structure. there are many interaction system could be induced into a systematic thermal interaction, include : ocean - continent system, basin - mountain interaction, superficial and mid - deep crust - mantle interaction, crust - mantle commingle interaction, vertical thermal interaction ( delamination ) etc.
依據地貌形態分為三類：正向穹窿型、負向塌陷型、邊隆核陷型：依據巖漿-熱力作用影響的深淺程度或深度分為五類： （古）地熱異常群集區、表淺層火山噴發-熱液活動與淺成侵入型、熱力背斜（熱穹窿） 、中深層侵入型、深部地幔（地殼）熱柱型；提出了熱力構造作用空間分佈的理想模式，將洋陸系統、盆山作用、淺表與中深部殼幔作用、殼幔混合、垂向熱力作用（拆沉）等納入一個整體統一的熱力作用系統中，為盆地動力學研究打開了一個新窗口；研討了熱力構造研究方法。For example, poly ( xylylviologendibromide ) and 4, 5 - bis ( 4 - methoxyphenyl ) - 2 - ( 4 - nitro - pheny ) imidazolium acetate di - hydrate ( c23h20n3o4 + c2h3o2 - 2h2o ), the hydration or dehydration of the crystal structure is related to the color charge of the crystal. the thermochromic schiff bases are the other family of compounds that show a self - isomerization induced by an intramolecular proton transfer from the hydroxyl oxygen to the imine nitrogen through the o - h. . n hydrogen bond, and they were observed thermochromism
利用液相法合成了兩種具有熱色性新的有機水合物， x射線單晶衍射確定了這兩種水合物的結構，利用uv 、 ir 、原位升溫紅外、原位升溫紫外、 tg - dsc探討了它們的變色機理。The path - way controlling of neptunium in co - decontamination step of purex process, the extraction thermodynamics of amido podand and its usage in recovery of actinides from simulated hllw have been investigated. more than 95 % np were maintained in np ( v ) in 1a extractor and flowed into 1 aw, if enough amount of hno2 was added in feed adjustment and then hno2 scavenger ( urea ) was added before extraction. three kinds of amido podand were synthesized, and the extraction of lanthanides, actinides and some fission products were studied. one of them ( tbopda, n, n, n ', n " - tetrabutyl - 3 - oxa - pantenadiamide ) was used as extractant to recover actinides from hllw. the results of experiments show that more than 99. 99 % actinides were recovered from hllw and separated basically in groups. the main digests are as follows : 1
鎿走向控制研究中通過調價階段加入亞硝酸、而萃取前清除亞硝酸的獨特辦法可以將大於95的鎿趕入1aw 。合成了三種酰胺莢醚萃取劑，研究了它們對錒系和裂片元素的萃取熱力學，通過條件實驗選擇了其中一種莢醚tbopda （ n ， n ， n 』 ， n 』 ?四丁基? 3 ?氧戊二酰胺） ，進行了從模擬高放廢液中分離錒鑭系元素的工藝研究，錒系的回收率大於99 . 99 ，並且基本上實現了錒鑭元素的組分離。其要點如下： 1The disperse degree of the ceramic can greatly affect uniformity of the composite, which limit the poling voltage and affect the piezoelectricity. in this paper, the relationships among constitutes, microstructures, dielectric and piezoelectric properties were calculated by employing the banno unit cell mode ; pzt ceramic were synthesized by the hydrothermal method and the appropriate solution was selected according the adsorption of pvdf on the ceramic particle surface ; then, relationships between the disperse degree and the fabrication process were studied. base on these, the pzt / pvdf composites intermingled some pan were prepared and the microstructures were investigated
論文首先利用bannounitcell模型，計算了pzt pvdf壓電復合材料的組成、結構、與其壓電和介電等性能之間的關系；針對壓電復合材料存在的均勻分散性差的缺點，選用水熱法制備的粒度均勻的pzt陶瓷粉末，並採用溶液混和法與聚合物pvdf進行分散復合，重點研究了不同工藝條件下陶瓷的均勻分散性及其與材料微觀結構之間的關系。Liquid - solid extrusion of composite material is a new kind of metal forming process, which has been developed in recent years with a promising practical application prospect for its simple working procedure, low cost and good workpiece performance. through a lot of experiments, the optimization and chosing method of key process parameters ( pouring temperature, mold warm - up temperature, impregnating pressure, impregnating time ) has been mastered. under the precondition of appropriate chosing these parameters, the effective control of extrusion velocity is the key of mading good workpiece. but the control of extrusion velocity remains a handwork, and it is heavily affected by such uncertainties as a handler ' s knowledge and skill about the process. in order to solve the problem, the automatic control of the extrusion velocity is studied, and a computer control system is also designed under existing condition
通過大量實驗，已掌握了關鍵工藝參數（熔液澆注溫度、擠壓模預熱溫度、浸漬時間、浸漬力）的優化選取方法。在合理選取關鍵工藝參數的前提下，擠壓速度的控制是成形出質量良好製件的關鍵。但是，目前對于擠壓速度的控制仍停留在手動控制階段，利用該工藝制備管、棒材製件的成功與否受操作者對該工藝及其設備的經驗及熟練程度等不確定因素影響很大。The main point can be summarized as follows : a low - temperature elemental - direct - reaction route to nanocrystalline cdse and znse, and further more, by using the newly produced se with high reactivity as reactant, a controllable synthetic route named " selenite reduction hydrothermal method " have been developed
在合成新途徑的探索方面，從發現了水熱元素直接反應法，發展到亞硒酸鹽水熱還原法，提出了化學調控合成的新概念，為液相中金屬硒碲化合物的合成提供了可能的動力學調控手段和方法。In this paper srco3 powders are first time synthesized successfully by low temperature solid state reaction with srcl2. 6h2o and ( nh4 ) 2co3. the size of srco3 is about 30 - 50nm. compared with liquid state method, this method produces little conglomeration and is easy to synthesize nanopowders
本論文根據低熱固相化學反應原理首次以srcl _ 2 ? 6h _ 2o和（ nh _ 4 ） _ 2co _ 3為原料成功合成了30 ? 50nm的srco _ 3粉體，克服了一般液相沉澱法易發生粉體團聚和難于制備納米級srco _ 3粉體的弊端，並通過研究找到了低熱固相反應終點的標志。Carbonyl iron particles and iron - epoxy resin composite particles, which both mrs and microwave absorber are based on, were prepared by method of dropping fe ( co ) 5 to dmf in constant temperatures and of heating the solution of fe ( co ) 5 / dmf stage by stage, combining in situ composite technique
本論文採用恆溫滴加法和逐步升溫液相法熱分解合成了羰基鐵粒子，並結合原位聚合復合技術制備了羰基鐵-環氧樹脂復合粒子，然後用它們組成了磁流變液和微波吸收材料。Aim : to analyze the mechanism, thermadynamic theoretical basis, dynamic mechanism and influencing factors of thermally induced phase separation ( tips ) in order to completely grasp the factors affecting the size, distribution and form of pores, so that the adjusted range of pore can be widened and the preparation of porous membrane can be repeated and controlled. methods : considering from the structural characteristics of tissue engineered materials, the methods of preparing porous membrane using tips technique, the hermadynamic theoretical basis, dynamic mechanism and influencing factors were analyzed, the problems and investigative directions in the future were also analyzed. tips technique is a process of phase separation of polymer homogenous solution under quenching, and it is suitable for diameter and structural form of the micropore materials prepared using tips are closely correlated with the kind and dispensing proportion of polymer attrnuant, polymer concentration and polymer molecular mass, etc. conducted, including determination of polymer - solvent system phase diagram, study of form and appearance of porous membrane of different thickness, study of form and appearance of porous membrane prepared with systems of different x, which is the parameter of polymer - solvent interaction
目的:分析熱致相分離成膜過程的機理、熱力學理論基礎、動力學機制以及影響因素，以便充分掌握影響孔度大小、分佈、形態的因素，使孔度調控范圍得以拓寬，使多孔膜的制備能重復可控.方法:從組織工程材料結構特點出發，分析熱致相分離聚合物多孔膜的制備方法及該法成膜的熱力學理論基礎、動力學機制以及影響因素.並分析實驗中存在的問題及今後的研究方向.結果:以熱致相分離法可制備聚合物多孔膜.熱致相分離法制備多孔膜是高聚物均相溶液在淬冷條件下發生相分離的過程，它適用於上臨界共溶溫度型聚合物一稀釋劑二元體系.熱致相分離法成膜的過程，可以認為是旋節線機理佔主導地位.熱致相分離法制備的微孔材料，其孔隙率、孔徑大小、結構形態與聚合物稀釋劑的種類、組成配比、聚合物濃度、聚合物分子量等因素密切相關.結論:可採用熱致相分離技術制備多孔膜，通過改變不同的成膜條件可獲得一系列不同孔徑尺寸和孔徑分佈的多孔膜材料.對熱致相分離成膜過程中聚合物-溶劑體系的相圖測定，不同厚度的多孔膜形貌研究，不同x （聚合物-溶劑相互作用參數）體系所制備的多孔膜形貌等需深人研究Under the guidance of synthetic information theory, the authors have quantitatively appraised the three types of gold deposits in the area using the method of logical information, that is, remelted - magmatic hydrothermal, syntecnic magmatic hydrothermal and volcanic sub volcanic hydrothermal gold deposits. 12 regions are predicted to be most perspective
在綜合信息成礦理論的指導下，對巖漿重熔熱液型金礦、巖漿同熔熱液型金礦床以及火山一次火山熱液型金礦床利用邏輯信息法進行了定量預測，總共預測出12個最有遠景的區域。This part emphasizes the synthesis of nanoarrays, aiming at controlling the size and distance of nanocrystallites using calixarene derivatives by altering the size, length and chemical structure of the organic molecules ; 2. this part emphasizes in situ synthesis strategy for fabrication of polymer network of zns based nanopowder, aiming at size controls, coating and preventing agglomeration following " one - pot " synthesis ; this method fits to low cost, large scale production ; 3. according to development in zno nanomaterials, we first report on the synthesis, characterization of amorphous zno, aiming at describing the principles and approaches of synthesis techniques, optical properties, spatial structure and doped effect ; the amorphous zno displays cage - like structure, showing a strong ultraviolet emission while the visible emission is nearly fully quenched, a potential uv - emission material ; 4
本論文以量子結構自組裝為出發點，提出利用杯芳烴及其衍生物的化學受限反應實現尺寸可調半導體納米粒子自組裝；提出有機聚合網路原位組裝zns基納米熒光粉方法，把熒光粉的納米化、包敷、防團聚在「一鍋」反應中完成，適于低成本，批量生產；根據當前zno的研究情況，我們首次合成了非晶zno ，研究了它的光學性質，確定了它的結構，並對其摻雜進行了初步的研究，非晶zno表現出強的深紫外發光特性，而可見發射非常弱，是一種有巨大潛在應用價值的深紫外發光材料；利用非晶zno的亞穩特性，對晶化過程中非晶zno納米晶zno三維受限量子結構特性，界面特性進行了深入的研究；利用固相熱分解一般受擴散控制特性，實現了尺寸可控的zno三維量子結構的自組裝；利用非晶zno的高度分散性，容易均勻成膜特性，實現了非晶籽晶誘導低溫液相外延自組裝生長高取向zno晶體薄膜。Through the analysis of the evolution of the microstructure, the honey comb at the grain boundary and the pool in the grain, furthermore according to the phase change thermodynamic and kinetics, the conclusions of the globalization mechanism and the reheating parameters were drawn as follows. 1
通過對半固態再結晶和半固態熔化過程中的組織轉變、晶界蜂巢及晶內液池現象的分析，結合相變熱力學和動力學原理，提出sima法制備鎂合金半固態球狀化組織的形成機制及工藝參數。Abstract : the technical characteristics, research status and recent progress in preparing nanometer particles by liquid - phase synthesis including precipitation, solvent evapration, hydrothermal, sol - gel and microemulsion technigues have been reviewed in the paper
文摘:論述了目前常用的液相合成技術（包括沉澱法、溶劑蒸發法、水熱法、溶膠-凝膠法和微乳液法）制備納米顆粒的技術特點、研究現狀及其進展。Cyanation of aryl halides is widely used in the synthesis of liquid crystals, but its traditional heating reactions require long time and high temperature
摘要鹵代芳烴的氰化反應在液晶單體合成中廣泛應用，但傳統的加熱方法反應時間長、溫度高。Therefore, a new technology, which consists of the mechanical milling ( mm ), reactive sintering and hot hydrostatic extrusion has been put forward
本文採用機械球磨?反應燒結?熱靜液擠壓方法，有望成為制備高性能ti - al基合金的有效途徑。Nano - cuo powders were successfully prepared by pressure - hydrothermal method with cuso4 5h2o and naoh as materials. xrd, sem and tem were used to characterize the samples. the influence of raw materials " initial concentration, thermal treatment " temperature, pressure and thermal treatment " time on the morphology and size of cuo were analyzed, and the possible growth mechanism was also discussed
以硫酸銅和氫氧化鈉為原料，用壓力-熱液法合成了納米氧化銅粉體，用xrd 、 sem 、 tem對所制得的氧化銅進行了觀察與表徵，分析了原料起始濃度、熱處理溫度、壓力、 ph值及熱處理時間對氧化銅形態和大小的影響，初步探討了不同形態氧化銅的生長機理。分享友人